反应条件
n-butyllithium in hexane byproducts: LiCl; suspn. of ZrCl4 in hexane under Ar cooled to -78°C, treated with BuLi in hexane, warmed to 20°C over 8 h, cooled to -78°C, treated with Cp for 1 h at -78°C, refluxed for 4 h, cooled; filtered, extd. with pentane-CH2Cl2, volatiles were removed under reduced pressure;
参考文献
Eisch, John J.; Owuor, Fredrick A.; Otieno, Peter O.
Organometallics, 2001 , vol. 20, # 20 p. 4132 - 4134
