反应条件
in tetrahydrofuran
(N2), added dropwise at room temp. in the dark, stirred 6 h, cooled at 0°C in the dark, added CoCp2 dropwise in 5 min., stirred 30 min.; precipitate filtered, dried in vac., soln. evaporated to dryness under vac. at room temp., recrystd. from hot EtOH, filtered, dried in vac.; elem. anal., IR;
参考文献
Calderazzo, Fausto; Marchetti, Fabio; Ungari, Fausto; Wieber, Markus
Gazzetta Chimica Italiana, 1991 , vol. 121, # 2 p. 93 - 100
