反应条件
in tetrahydrofuran byproducts: CH4; Heating of equimolar amts. of starting compds. (THF, Ar, 17 h).; Cooling, filtn., drying in vac. Recrystn. by washing of solid residue (cold toluene), dissolving in THF and keeping of soln. at -78°C. Filtn., washing (cold hexane), vac.-drying, elem. anal.;
参考文献
Selent, Detlef; Pickardt, Joachim; Claus, Peter
Journal of Organometallic Chemistry, 1994 , vol. 468, # 1-2 p. 131 - 138
