双(2-氯乙基)氨基磷酰二氯合成路线 (共 51 条)
反应条件
triethylamine in 1,4-dioxane
参考文献
Zimmer,H.; Sill,A.D.
Arzneimittel Forschung, 1964 , vol. 14, p. 150 - 151
反应条件
1: in toluene
T=0°C; 0.333333 h;
2: With triethylamine in toluene
T=20°C; 9 h; Reflux;
参考文献
Chen, Xiaolan; Yuan, Jinwei; Wang, Junliang; Qu, Lingbo; Yu, Zhangqi; Zhao, Yufen
Journal of Chemical Research, 2010 , # 7 p. 407 - 409
反应条件
triethylamine in phosphorus(III) oxychloride; toluene
参考文献
Board of Regents, University of Texas System
Patent: US4841085 A1, 1989 ;
反应条件
triethylamine in dichloromethane
参考文献
Farmer; Cox
Journal of Medicinal Chemistry, 1975 , vol. 18, # 11 p. 1106 - 1110
反应条件
triethylamine in ethyl acetate
参考文献
Ludeman,S.M.; Zon,G.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 12 p. 1251 - 1253
反应条件
triethylamine in ethyl acetate
参考文献
Ludeman,S.M.; Zon,G.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 12 p. 1251 - 1253
反应条件
triethylamine in ethyl acetate
Ambient temperature;
参考文献
Ludeman,S.M.; Zon,G.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 12 p. 1251 - 1253
反应条件
triethylamine in toluene
T=35 - 45°C; 4 h;
参考文献
Rao, L. Nagaprasada; Reddy, C. Devendranath; Reddy, V. Krishna; Hagar, Jacob D.; Tran, Kevin; Berlin, K. Darrell
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 2 p. 399 - 410
反应条件
triethylamine in toluene
20 h; RefluxLarge scale;
参考文献
Herr, R. Jason; Zhichkin, Paul; Hernandez-Abad, Pedro E.; Meckler, Harold; Schow, Steven R.
Organic Process Research and Development, 2001 , vol. 5, # 4 p. 442 - 444
反应条件
triethylamine in dichloromethane
72 h; Ambient temperature;
参考文献
Wan, Huijie; Modro, Tomasz A.
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 155 - 168