O,O,O-三乙基硫代磷酸酯合成路线 (共 68 条)
反应条件
DTD in acetonitrile T=20°C;
参考文献
Song, Quanlai; Wang, Zhiwei; Sanghvi, Yogesh S.
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 5-8 p. 629 - 633
反应条件
thiamine diphosphate; diethylazodicarboxylate in benzene T=35 - 40°C; 6 h; Yield given;
参考文献
Mlotkowska, B.; Wartalowska-Graczyk, M.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 4 p. 735 - 740
反应条件
sulfur trioxide in dichloromethane T=-78°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 11 p. 3495 - 3499
反应条件
dicyclohexyl-carbodiimide in diethyl ether 240 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 49, # 5 p. 899 - 908
反应条件
in ethanol T=20°C; 14 h;
参考文献
Rung, Bruno; Schwack, Wolfgang
Journal of Agricultural and Food Chemistry, 2005 , vol. 53, # 23 p. 9140 - 9145
反应条件
di-tert-butyl peroxide T=140°C;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1243,1247
反应条件
triethyl phosphite in acetonitrile 16 h; Irradiation;
参考文献
Tsujimoto, Kazuo; Okeda, Yukihiro; Ohashi, Mamoru
Journal of the Chemical Society, Chemical Communications, 1985 , # 24 p. 1803 - 1804
反应条件
in 1,2-dichloro-ethane T=20°C; 0.0833333 h;
参考文献
Kamer; Roelen; Van den Elst; Van der Marel; Van Boom
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6757 - 6760
反应条件
in diethyl ether T=0°C; 0.25 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 4 p. 847 - 849,736 - 738
反应条件
in 1-n-butyl-3-methylimidazolium tetrafluoroborate T=80°C; 2 h; Ionic liquid; Product distribution / selectivity;
参考文献
THE QUEEN'S UNI.IONIC LIQUID LAB. RESEARCH CENTRE
Patent: WO2007/20473 A1, 2007 ;
Location in patent: Page/Page column 29-30 ;