2-乙基-2-甲基-1,3-二氧杂烷合成路线 （共 20 条）
反应条件
[CuI4CuII(mtpo)4(H2O)2Cl2]n in toluene T=110°C; 24 h;
参考文献
Inorganic Chemistry Communications, , vol. 22, p. 73 - 76
反应条件
NafionTMS T=70°C; acetalisation; 20 h;
参考文献
Synthetic Communications, , vol. 29, # 22 p. 4035 - 4042
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 173 - 178
反应条件
1: toluene-4-sulfonic acid / Entfernen des entstehenden Butanons 2: aqueous methanol. NaOH-solution 3: diethyl ether View Scheme
参考文献
Warren; Weedon
Journal of the Chemical Society, 1958 , p. 3972,3978
反应条件
toluene-4-sulfonic acid Entfernen des entstehenden Butanons;
参考文献
Warren; Weedon
Journal of the Chemical Society, 1958 , p. 3972,3978
反应条件
toluene-4-sulfonic acid
参考文献
Searle and Co.
Patent: US2875215 , 1957 ;
反应条件
diisobutylaluminium hydride; benzene Behandeln einer Loesung des erhaltenen Diisobutylaluminium-<2-sec-butoxy-aethylats> in Aether mit wss.Schwefelsaeure;
参考文献
Sacharkin; Chorlina
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 2255;engl.Ausg.S.2156
反应条件
triethylaluminum; diethyl aluminium hydride in hexane; kerosene 20 h; Heating;
参考文献
Journal of applied chemistry of the USSR, , vol. 58, # 7 pt 1 p. 1419 - 1423
反应条件
diethyl aluminium hydride in hexane; kerosene 40 h; Heating;
参考文献
Journal of applied chemistry of the USSR, , vol. 58, # 7 pt 1 p. 1419 - 1423
反应条件
toluene-4-sulfonic acid
参考文献
Caspi
Journal of Organic Chemistry, 1956 , vol. 21, p. 729,731
Full Text Show Details
Bowers; Ringold
Journal of the American Chemical Society, 1959 , vol. 81, p. 3710
