2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
manganese(IV) oxide; In(OSO2CF3)3 in dichloromethane
T=20°C; 24 h;
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4891 - 4894
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide
T=20°C; 70 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide
T=20°C; 39 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide
T=20°C; 42 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
polystyrene divinyl benzene sulfonic acid in dichloromethane
T=20 - 50°C; chemoselective reaction;
参考文献
Verma, Sanjeev K.; Sathe, Manisha; Kaushik
Synthetic Communications, 2010 , vol. 40, # 11 p. 1701 - 1707
反应条件
1.1: 94 percent / CF3COOH / toluene / 15 h / 90 °C
2.1: Mg / tetrahydrofuran / 2 h / 60 °C
2.2: 62 percent / tetrahydrofuran / 15 h / 0 °C
View Scheme
参考文献
Querner, Claudia; Reiss, Peter; Bleuse, Joel; Pron, Adam
Journal of the American Chemical Society, 2004 , vol. 126, # 37 p. 11574 - 11582
参考文献
Qiao, Zeng-Ying; Du, Fu-Sheng; Zhang, Rui; Liang, De-Hai; Li, Zi-Chen
Macromolecules, 2010 , vol. 43, # 15 p. 6485 - 6494
反应条件
1: toluene-4-sulfonic acid / toluene / 135 - 140 °C / |Dean-Stark
2: hydrogen; palladium 10 on activated carbon / methanol / 760.05 Torr
View Scheme
参考文献
Tai, Vincent W.-F.; Garrido, Dulce; Price, Daniel J.; Maynard, Andrew; Pouliot, Jeffrey J.; Xiong, Zhiping; Seal, John W.; Creech, Katrina L.; Kryn, Luz H.; Baughman, Todd M.; Peat, Andrew J.
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 10 p. 2288 - 2294
反应条件
4-fluorophenyl boronic acid; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 38 h;
参考文献
Maki, Toshihide; Ushijima, Nobuto; Matsumura, Yoshihiro; Onomura, Osamu
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1466 - 1468
反应条件
potassium tert-butylate in 1,4-dioxane
T=90°C; 2 h;
参考文献
Kalesse, Markus; Quitschalle, Monika; Claus, Eckhard; Gerlach, Kai; Pahl, Axel; Meyer, Hartmut H.
European Journal of Organic Chemistry, 1999 , # 11 p. 2817 - 2823
