2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
sulfuric acid
T=20°C; Condensation; 1 h;
参考文献
Romero, Jordi; Ventura, Francesc; Caixach, Josep; Rivera, Josep; Gode, Llui Xavier; Ninerola, Josep Ma.
Environmental Science and Technology, 1998 , vol. 32, # 2 p. 206 - 216
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
chloro-trimethyl-silane
T=20°C; 0.416667 h; also other catalyst was used (H3PO3); in ether; without Me3SiCl;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Larionov, V. I.; Zlot-skii, S. S.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1394 - 1401,1229 - 1236
反应条件
1: 68 percent / toluene / 0.25 h
2: 91 percent / H2SO4 / heptane / 1.5 h / 20 °C
View Scheme
参考文献
Gvozdik; Gal'chenko; Musavirov
Russian Journal of General Chemistry, 1996 , vol. 66, # 5 p. 784 - 787
反应条件
sulfuric acid
T=20°C; Condensation; 1 h;
参考文献
Romero, Jordi; Ventura, Francesc; Caixach, Josep; Rivera, Josep; Gode, Llui Xavier; Ninerola, Josep Ma.
Environmental Science and Technology, 1998 , vol. 32, # 2 p. 206 - 216
反应条件
1: 68 percent / toluene / 0.25 h
2: 75 percent / para-toluenesulfonic acid / heptane / 1.5 h / 20 °C
View Scheme
参考文献
Gvozdik; Gal'chenko; Musavirov
Russian Journal of General Chemistry, 1996 , vol. 66, # 5 p. 784 - 787
反应条件
toluene-4-sulfonic acid in toluene
Heating;
参考文献
Demchuk; Lazareva; Lindeman; Khrustalyov; Struchkov; Ismagilov; Troyansky; Nikishin
Synthesis, 1995 , # 3 p. 307 - 311
反应条件
polyacrylonitrile hybrid fiber mat supported solid acid catalyst in cyclohexane
Reflux;
参考文献
Shao, Linjun; Du, Yijun; Xing, Guiying; Lv, Weixi; Liang, Xuezheng; Qi, Chenze
Monatshefte fur Chemie, 2012 , vol. 143, # 8 p. 1199 - 1203
反应条件
camphor-10-sulfonic acid in dichloromethane
Inert atmosphere;
参考文献
Brozek, Laura A.; Sieber, Joshua D.; Morken, James P.
Organic Letters, 2011 , vol. 13, # 5 p. 995 - 997
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=20°C; 0.5 h;
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
