2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
参考文献
Klimovitskii, E. N.; Sergeeva, G. N.; Timirbaev, M. B.; Arbuzov, B. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 2 p. 216 - 219
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 2 p. 295 - 299
参考文献
Klimovitskii, E. N.; Sergeeva, G. N.; Timirbaev, M. B.; Arbuzov, B. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 2 p. 216 - 219
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 2 p. 295 - 299
反应条件
1: With amberlyst-15 in benzene
15 h; Heating;
2: With sodium hydroxide in water
0.5 h; Heating;
参考文献
Balakumar, Arumugham; Muthukumaran, Kannan; Lindsey, Jonathan S.
Patent: US2005/277770 A1, 2005 ;
Location in patent: Page/Page column 10 ;
反应条件
1: 2,2,6,6-tetramethyl-piperidine; benzonitrile With n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran
T=-78 - 20°C;
2: 3-hydroxy-2,2-dimethylpropanol in toluene
T=20°C;
参考文献
Kristensen, Jesper; Lysen, Morten; Vedso, Per; Begtrup, Mikael
Organic Letters, 2001 , vol. 3, # 10 p. 1435 - 1437
反应条件
2: NaI
3: KOH
4: saponification
5: 180 °C
6: LiAlH4
View Scheme
参考文献
Park; Varick; Newcomb
Tetrahedron Letters, 1990 , vol. 31, # 21 p. 2975 - 2978
反应条件
pyridine in diethyl ether
参考文献
Singh,G.
Journal of Organic Chemistry, 1979 , vol. 44, p. 1060 - 1063
反应条件
1H-tetrazole in toluene; acetonitrile
T=20°C;
参考文献
Renard, Pierre-Yves; Vayron, Philippe; Mioskowski, Charles
Organic Letters, 2003 , vol. 5, # 10 p. 1661 - 1664
参考文献
Arshinova,R.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, # 7 p. 1408 - 1412
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 7 p. 1518 - 1522
反应条件
potassium hydroxide in N,N-dimethyl-formamide
-78 to 30...80 deg C;
参考文献
Sievert, Allen C.; Tong, Walter R.; Nappa, Mario J.
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 397 - 418
参考文献
Romero, Jordi; Ventura, Francesc; Caixach, Josep; Rivera, Josep; Gode, Llui Xavier; Ninerola, Josep Ma.
Environmental Science and Technology, 1998 , vol. 32, # 2 p. 206 - 216
