2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
in benzene 4-formylphenylboronic acid and 2,2-dimethylpropane-1,3-diol were refluxed in benzene for 2 h 30 min; soln. was evapd. to dryness;
参考文献
Dixon; Collin; Sauvage; Flamigni
Inorganic Chemistry, 2001 , vol. 40, # 22 p. 5507 - 5517
反应条件
1: potassium acetate / 80 °C 2: tetrakis(triphenylphosphine) palladium(0) / toluene / 22 h / 80 °C View Scheme
参考文献
Bello, Charles S.; Schmidt-Leithoff, Joachim
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6230 - 6235,6
反应条件
sodium hydroxide 0.0208333 h; microwave irradiation;
参考文献
Rajabi, Fatemeh
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 395 - 397
反应条件
acyl transferase from Mycobacterium smegmatis in aq. phosphate buffer T=20°C; pH=8; 0.5 h; Enzymatic reaction; ConcentrationpH-valueTime;
参考文献
Wiermans, Lotte; Hofzumahaus, Sebastian; Schotten, Christiane; Weigand, Lisa; Schallmey, Marcus; Schallmey, Anett; De Maria, Pablo Dominguez
ChemCatChem, 2013 , vol. 5, # 12 p. 3719 - 3724
反应条件
1: PBr3 / 150 °C 2: glacial acetic acid / 150 °C View Scheme
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
反应条件
indium (III) fluoride in toluene 3.5 h; Reflux; chemoselective reaction;
参考文献
Madabhushi, Sridhar; Mallu, Kishore Kumar Reddy; Chinthala, Narsaiah; Beeram, China Ramanaiah; Vangipuram, Venkata Sairam
Tetrahedron Letters, 2012 , vol. 53, # 6 p. 697 - 701
反应条件
trimethyl orthoformate; aminopropylated Silica-Gel hydrochloride (APSG*HCl) resin 10 h; Ambient temperature; Yields of byproduct given;
参考文献
Gasparrini, F.; Giovannoli, M.; Misiti, D.; Palmieri, G.
Tetrahedron, 1984 , vol. 40, # 9 p. 1491 - 1500
反应条件
dimethyl-dichlorosilane in tetrahydrofuran; dichloromethane 0.5 h; Ambient temperature;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Sugiyama, Yoshie; Fukata, Fumio; Haruta, Jun-ichi; Yasumitsu, Tamura
Tetrahedron Letters, 1983 , vol. 24, # 12 p. 1273 - 1276
反应条件
in 1,4-dioxane T=20°C; 0.166667 h;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Lapuka, L. F.; Kantor, E. A.; Sarmanaev, R. S.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 6 p. 670 - 675
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 6 p. 845 - 851
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
