2,2-二甲基-1,3-丙二醇合成路线 (共 467 条)
反应条件
(neocuproine)Pd(OAc)2; NaDCC in acetonitrile T=35°C; P=1794.37 Torr; 18 h;
参考文献
Pearson, David M.; Conley, Nicholas R.; Waymouth, Robert M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 16 p. 3007 - 3013
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=70°C; P=7500.75 Torr; 18 h; Autoclave;
参考文献
Lim, Yu Na; Lee, Chan; Jang, Hye-Young
European Journal of Organic Chemistry, 2014 , vol. 2014, # 9 p. 1823 - 1826
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane 3 h; Ambient temperature;
参考文献
Kim, Sunggak; Ko, Young Kwan
Heterocycles, 1986 , vol. 24, # 6 p. 1625 - 1630
反应条件
triethylamine in tetrahydrofuran
参考文献
Al-Azemi, Talal F.; Dib, Hicham H.; Al-Awadi, Nouria A.; El-Dusouqui, Osman M.E.
Tetrahedron, 2008 , vol. 64, # 18 p. 4126 - 4134
反应条件
in dichloromethane; toluene
参考文献
Bayer Aktiengesellschaft
Patent: US5023346 A1, 1991 ;
反应条件
potassium hydroxide 1 h; Heating;
参考文献
Dale, Johannes; Fredriksen, Siw B.
Acta Chemica Scandinavica, 1991 , vol. 45, # 1 p. 82 - 91
反应条件
[14C]-Antipyrine; chloroform; toluene
参考文献
Ludwig; Piech
Journal of the American Chemical Society, 1951 , vol. 73, p. 5779
参考文献
Sarel; Pohoryles
Journal of the American Chemical Society, 1958 , vol. 80, p. 4596,4598
反应条件
pyridine; dichlorotriphenylphosphorane in chloroform 12 h; Ambient temperature;
参考文献
Acta Chemica Scandinavica, , vol. 45, # 1 p. 82 - 91
反应条件
1: 96 percent / pyridine 2: 71 percent / ethane-1,2-diol / 2 h / Heating View Scheme
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 2 p. 505 - 509