2,2-二甲基-1,3-丙二醇合成路线 (共 467 条)
参考文献
Monatshefte fuer Chemie, , vol. 21, p. 301
参考文献
Monatshefte fuer Chemie, , vol. 21, p. 313
参考文献
Monatshefte fuer Chemie, , vol. 21, p. 301
反应条件
1: hydrobromic acid / 100 °C 2: sodium amalgam; water; methanol View Scheme
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
反应条件
1: hydrobromic acid / 100 °C 2: sodium amalgam; water; methanol 3: chromic acid View Scheme
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
参考文献
Brannock; Lappin
Journal of the American Chemical Society, 1955 , vol. 77, p. 6052
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Searles et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1770,1773
反应条件
potassium hydroxide 18 h; Ambient temperature;
参考文献
Wilson, Michael W.; Hodges, John C.
Organic Preparations and Procedures International, 1993 , vol. 25, # 6 p. 665 - 672
反应条件
Novozyme 435 in 1,1-dimethylpropan-1-ol T=50°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction;
参考文献
Popescu, Dragos; Hoogenboom, Richard; Keul, Helmut; Moeller, Martin
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 12 p. 2610 - 2621
反应条件
1: 92 percent / NEt3 / tetrahydrofuran / -78 deg C to RT, overnight 2: 43 percent / dimethylsulfoxide / 168 h / 85 - 90 °C View Scheme
参考文献
Equi, Angela M.; Brown, Alison M.; Cooper, Alan; Her, Surjit K.; Watson, Allan B.; Robins, David J.
Tetrahedron, 1991 , vol. 47, # 3 p. 507 - 518
反应条件
sodium hydrogencarbonate in ethylene glycol dimethyl ether
参考文献
Newman,M.S.; Kilbourn,E.
Journal of Organic Chemistry, 1970 , vol. 35, p. 3186 - 3188