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结构式
乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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125345-27-9
合成路线
（共 10 条）
125345-26-8
→
反应条件
125345-27-9
反应条件
oxalic acid in methanol; water 2 h; Heating; Yield given;
参考文献
Okamoto, Ryuichi; Okazaki, Eri; Noguchi, Keiichi; Tanaka, Ken
Organic Letters, 2011 , vol. 13, # 18 p. 4894 - 4897
533-58-4
2-碘苯酚
+
693-02-7
1-己炔
→
反应条件
125345-27-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=0 - 20°C; Sonogashira Cross-Coupling; 5 h; Inert atmosphere;
参考文献
Lee, Euichul; Ryu, Taekyu; Park, Youngchul; Park, Sangjune; Lee, Phil Ho
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1585 - 1596
80778-47-8
1-碘-2-(甲氧基甲氧基)苯
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反应条件
125345-27-9
反应条件
1: Et2NH / PdCl2(PPh3)2, CuI / 12 h / Ambient temperature 2: conc. HCl / methanol / 24 h / Ambient temperature View Scheme
参考文献
Okamoto, Ryuichi; Okazaki, Eri; Noguchi, Keiichi; Tanaka, Ken
Organic Letters, 2011 , vol. 13, # 18 p. 4894 - 4897
693-02-7
1-己炔
→
反应条件
125345-27-9
反应条件
1: Et2NH / PdCl2(PPh3)2, CuI / 12 h / Ambient temperature 2: conc. HCl / methanol / 24 h / Ambient temperature View Scheme
参考文献
Okamoto, Ryuichi; Okazaki, Eri; Noguchi, Keiichi; Tanaka, Ken
Organic Letters, 2011 , vol. 13, # 18 p. 4894 - 4897
533-58-4
2-碘苯酚
→
反应条件
125345-27-9
反应条件
1: NaH / 5 h / Ambient temperature 2: Et2NH / PdCl2(PPh3)2, CuI / 12 h / Ambient temperature 3: conc. HCl / methanol / 24 h / Ambient temperature View Scheme
参考文献
Sun, Shi-Xin; Wang, Jun-Jie; Xu, Zi-Jun; Cao, Lu-Ya; Shi, Zi-Fa; Zhang, Hao-Li
Tetrahedron, 2014 , vol. 70, # 24 p. 3798 - 3806
1244030-03-2
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反应条件
125345-27-9
反应条件
ammonia in water T=20°C;
参考文献
Sen, Subhabrata; Kulkarni, Parag; Borate, Kailaskumar; Pai, Nandini R.
Tetrahedron Letters, 2009 , vol. 50, # 28 p. 4128 - 4131
125345-27-9
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反应条件
4265-27-4
2-丁基苯并呋喃
反应条件
1: With N,N,N',N,-tetramethylethylenediamine; diethylzinc in toluene T=120°C; 1 h; 2: With ammonium chloride in toluene
参考文献
Nakamura, Masaharu; Ilies, Laurean; Otsubo, Saika; Nakamura, Eiichi
Angewandte Chemie - International Edition, 2006 , vol. 45, # 6 p. 944 - 947
125345-27-9
→
反应条件
4265-27-4
2-丁基苯并呋喃
+
1244029-99-9
+
1244029-98-8
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; water; P[(2,6-OMe)2C6H3]3; lithium chloride in 1,4-dioxane T=90°C; 24 h;
参考文献
Boyer, Alistair; Isono, Naohiro; Lackner, Sebastian; Lautens, Mark
Tetrahedron, 2010 , vol. 66, # 33 p. 6468 - 6482
930-68-7
2-环己烯-1-酮
+
125345-27-9
→
反应条件
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; [Rh(OH)(cycloocta-1,5-diene)]2; water; lithium chloride in 1,4-dioxane T=90°C; 6 h;
参考文献
Boyer, Alistair; Isono, Naohiro; Lackner, Sebastian; Lautens, Mark
Tetrahedron, 2010 , vol. 66, # 33 p. 6468 - 6482
201230-82-2
+
125345-27-9
→
反应条件
66898-41-7
反应条件
water; triethylamine; Rh6(CO)12 in 1,4-dioxane T=175°C; P=76000 Torr; 3 h;
参考文献
Yoneda, Eiji; Sugioka, Takashi; Hirao, Kojiro; Zhahg, Shi-Wei; Takahashi, Shigetoshi
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 3 p. 477 - 483
