1,3-二(3-硝基苯基)脲合成路线 （共 3 条）
反应条件
hydrogenchloride; water; iron in ethanol T=95°C; 1.5 h;
参考文献
Radi, Marco; Falchi, Federico; Garbelli, Anna; Samuele, Alberta; Bernardo, Vincenzo; Paolucci, Stefania; Baldanti, Fausto; Schenone, Silvia; Manetti, Fabrizio; Maga, Giovanni; Botta, Maurizio
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 5 p. 2094 - 2098
反应条件
sodium hydroxide; phenylmethyltriethylammonium bromide in water; benzene
T=55°C; 48 h;
参考文献
Nolte,R.J.; Cram,D.J.
Journal of the American Chemical Society, 1976 , vol. 106, p. 1416
反应条件
1: 40 percent / benzyltriethylammonium bromide, NaOH / benzene; H2O / 48 h / 55 °C
2: 70 percent / iron, conc. HCl / ethanol; H2O / 4 h / Heating
View Scheme
参考文献
Nolte,R.J.; Cram,D.J.
Journal of the American Chemical Society, 1976 , vol. 106, p. 1416
