反应条件
1: 70 percent / periodic acid / H2O; methanol
2: 23 percent / calcium oxide / H2O / 1.) 3 h, room temperature, 2.) 35 h, 70-80 deg C
3: 79 percent / triethylphosphite, triethylamine / ethanol / Heating
4: 86 percent / sulphuryl chloride / CHCl3 / 2 h
View Scheme
参考文献
Edmundson, R. S.; Forth, C. I.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 315 - 320