4,4′-二甲氧基苯偶酰合成路线 （共 154 条）
反应条件
1.1: KOH / ethanol 2.1: Mg / tetrahydrofuran 2.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran 3.1: SeO2; 90 percent aq. AcOH; H2SO4 View Scheme
参考文献
Journal of Materials Chemistry, , vol. 11, # 4 p. 1063 - 1071
反应条件
1.1: thionyl chloride / 3 h / Reflux 1.2: 3 h / 20 °C 2.1: selenium(IV) oxide / dimethyl sulfoxide / 3.5 h / 100 °C View Scheme
参考文献
US2012/225863 A1, ;
US 20120225863 A1
反应条件
1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 0 °C / |Inert atmosphere 1.2: 4 h / 20 °C / |Inert atmosphere 2.1: hydrogen / methanol / 5 h / 3620.13 Torr / |Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 39 p. 5327 - 5330
反应条件
1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 0 °C / |Inert atmosphere 1.2: 4 h / 20 °C / |Inert atmosphere 2.1: hydrogen / methanol / 5 h / 3620.13 Torr / |Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 39 p. 5327 - 5330
反应条件
1: Grubb's 2nd generation catalyst / toluene / 1.5 h / 80 °C / |Inert atmosphere 2: Grubb's 2nd generation catalyst; tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / toluene; acetonitrile; water / 1 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 11 p. 5427 - 5435
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 6 p. 514 - 517
反应条件
manganese triacetate; lithium chloride in acetic acid 1.51667 h; Heating; Product distributionMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 1 p. 142 - 145
反应条件
sodium hydroxide; selenium(IV) oxide 1.) DMF, 78-80 deg C; 2.) THF, r.t.; Yield given. Multistep reaction;
参考文献
Synlett, , vol. 1997, # 6 p. 671 - 672
反应条件
in acetonitrile Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 26, # 6 p. 789 - 792
反应条件
in acetonitrile Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 26, # 6 p. 789 - 792
