4,4′-二甲氧基苯偶酰合成路线 (共 154 条)
反应条件
tetra-n-butylammonium perchlorate in acetonitrile Electrolysis;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 4 p. 755 - 756
反应条件
1: 72 percent / SmI2 / tetrahydrofuran / 19 h / Heating 2: HCl / 14 h View Scheme
参考文献
Chemistry Letters, , vol. 33, # 2 p. 102 - 103
反应条件
1.1: sodium hydroxide / ethanol; water / 20 °C 1.2: 0 - 20 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 3.1: sodium hypochlorite; water / dichloromethane / 4 h / 20 °C 4.1: water; acetic acid / 0.5 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 3 p. 733 - 735
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 2: sodium hypochlorite; water / dichloromethane / 4 h / 20 °C 3: water; acetic acid / 0.5 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 3 p. 733 - 735
反应条件
1: sodium hypochlorite; water / dichloromethane / 4 h / 20 °C 2: water; acetic acid / 0.5 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 3 p. 733 - 735
反应条件
Grubb's 2nd generation catalyst; tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; toluene; acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
lead(IV) acetate; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 62, p. 1601
Journal of Biological Chemistry, , vol. 146, p. 395
反应条件
dimethyl sulfoxide 0.05 h; Irradiation;
参考文献
Villemin; Hammadi
Synthetic Communications, 1995 , vol. 25, # 20 p. 3145 - 3148
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) 0 deg C, 1 h, 2.) 0 deg C, 1 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 17 p. 4988 - 4992
反应条件
1: Perkin condensation 2: 19 percent / manganese(III)acetate, LiCl / acetic acid / 2.67 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 3153 - 3160