1,1,3,3-四乙氧基丙烷合成路线 （共 75 条）
反应条件
1: With boron trifluoride diethyl etherate T=20 - 38°C; 2: With potassium carbonate T=20°C; 2 h;
参考文献
UCHREZHDENIE ROSSIISKOI AKADEMII NAUK INSTITUT MOLEKULYARNOI BIOLOGII IM. V.A. ENGELGARDTA RAN (IMB RAN)
Patent: EP2157088 A1, 2010 ;
Location in patent: Page/Page column 54-55 ;
反应条件
boron trifluoride diethyl etherate in diethyl ether T=10°C;
参考文献
Helvetica Chimica Acta, , vol. 71, p. 1 - 23
反应条件
anhydrous iron chloride T=-30°C; 6 h; Product distribution / selectivity;
参考文献
EP1607381 A1, ;
Page/Page column 6 ;
反应条件
zinc(II) chloride in ethyl acetate 3 h; Ambient temperature;
参考文献
Makin, S. M.; Kruglikova, R. I.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 630 - 634
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 723 - 727
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2660
反应条件
iron(III) chloride; sodium hydrogencarbonate 1) 2 h, reflux; 2) 20 deg C, 2 h;
参考文献
Yatluk, Yu. G.; Suvorov, A. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 316 - 320
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 376 - 381
反应条件
zinc(II) chloride in diethyl ether temperature below 30 deg C;
参考文献
Imashev, U. B.; Kalashnikov, S. M.; Gordeeva, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 4 p. 369 - 373
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 4 p. 459 - 463
反应条件
p-benozquinone T=30°C; 24 h;
参考文献
US6355844 B1, ;
Example 6 ;
反应条件
P=8826.09 - 12503.6 Torr;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 4607
Org. Synth. Coll. Vol., , vol. IV, p. 801
反应条件
hydrogenchloride; ozone -40 deg C, then ca. 30 min reflux;
参考文献
Mittelbach, Martin; Poklukar, Norbert; Junek, Hans
Liebigs Annalen der Chemie, 1990 , # 2 p. 185 - 188
