1,3-双(4-氯苯基)尿素合成路线 （共 117 条）
反应条件
T=160 - 230°C; ΔH; heat of dissociation; Thermodynamic data;
参考文献
Chimishkyan, A. L.; Svetlova, L. P.; Leonova, T. V.; Gluyaev, N. D.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 7 p. 1477 - 1481,1317 - 1320
参考文献
Chattaway; Orton
Chemische Berichte, 1901 , vol. 34, p. 1080
反应条件
T=121.15 - 152.65°C; KineticsActivation energy;
参考文献
Mantrov; Chimishkyan
Russian Journal of Physical Chemistry A, 2002 , vol. 76, # 5 p. 738 - 741
反应条件
oxygen; PdCl2(p-ClC6H4NH2)2 in methanol
T=80°C; 6 h;
参考文献
Giannoccaro, Potenzo
Journal of Organometallic Chemistry, 1987 , vol. 336, p. 271 - 278
反应条件
4-(N,N-dimethlyamino)pyridine in toluene
T=80 - 90°C; 6 h;
参考文献
CHEMAGIS LTD.; PERRIGO COMPANY
Patent: WO2007/70804 A2, 2007 ;
Location in patent: Page/Page column 21-22 ;
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine) in 1,4-dioxane
T=100°C; 2 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
potassium phosphate; 1,2-diamino-cyclohexane; copper(l) iodide in N,N-dimethyl-formamide
T=80°C; 24 h;
参考文献
Nandakumar, Mecheril V.
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1989 - 1990
反应条件
iodine
T=90 - 95°C; 0.0833333 h;
参考文献
Pasha; Madhusudana Reddy
Synthetic Communications, 2009 , vol. 39, # 16 p. 2928 - 2934
反应条件
tin(IV) chloride; triethylamine; [Pt(triphenylphosphine)2Cl2] in benzene
T=140°C; 4 h;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1985 , vol. 290, p. 249 - 256
反应条件
tert.-butylhydroperoxide; copper(I) bromide in water
T=20 - 80°C; under open air;
参考文献
Wei, Ying; Ding, Hongqian; Lin, Shaoxia; Liang, Fushun
Organic Letters, 2011 , vol. 13, # 7 p. 1674 - 1677
