反应条件
in tetrahydrofuran Ar atmosphere, addn. of Rh complex to soln. of Cr complex and P4, stirring (room temp., 10 min), concn. to dryness (70°C, vacuum); sublimation (50°C, vacuum), suspn. (n-pentane), filtration, extn.with hot filtrate, concn. (vacuum), crystn. (5°C), sublimation ( 60°C, vacuum), crystn. (CH2Cl2, 0°C), dissolution of extd.solid (CH2Cl2), crystn. (0°C);
参考文献
Chemische Berichte, , vol. 128, # 3 p. 251 - 258
