反应条件
Zn in hydrogenchloride; ethanol byproducts: Zn(2+); Electrochem. Process; in cell with Pb cathode and Zn anode; P4 suspended in H2O/EtOH (2:1), warmed to 60°C under N2; 0.5 mL 2 M HCl added; current (150 mA) applied for 30 min, 1.5 mL HCl added, stirred at 60°C; detd. by (14)P NMR;
参考文献
Yakhvarov, Dmitry; Caporali, Maria; Gonsalvi, Luca; Latypov, Shamil; Mirabello, Vincenzo; Rizvanov, Ildar; Sinyashin, Oleg; Stoppioni, Piero; Peruzzini, Maurizio
Angewandte Chemie - International Edition, 2011 , vol. 50, # 23 p. 5370 - 5373