反应条件
CO in tetrahydrofuran byproducts: Na(C5H5); absence of air and moisture; treatment of V-complex with 1 atm CO for 30min (room temp.), addn. of 1 equiv. Na-sand, stirring under 1 atm CO fo r 12 h; evapn., sublimation;
参考文献
Fachinetti, Giuseppe; Nero, Stefano Del; Floriani, Carlo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1046 - 1049