4-氯-3-硝基三氟甲苯合成路线 （共 136 条）
反应条件
sulfuric acid; nitric acid
参考文献
Zhou, Xinming; He, Yantao; Wang, Miao; Ding, Yixiang
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 3 p. 651 - 659
反应条件
1: 1-amino-3-nitro-4-chlorobenzene With hydrogenchloride in water T=0°C; 0.0833333 h; Inert atmosphereSchlenk technique; 2: With tert.-butylnitrite T=0°C; 0.25 h; Inert atmosphereSchlenk technique; 3: trifluoromethylsilver T=-78 - 20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xi; Xu, Yan; Mo, Fanyang; Ji, Guojing; Qiu, Di; Feng, Jiajie; Ye, Yuxuan; Zhang, Songnan; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 28 p. 10330 - 10333
反应条件
1: anhydrous HF / 110 °C / 7355.08 - 10297.1 Torr 2: Nitrierung View Scheme
反应条件
potassium fluoride; phthalolyl chloride; anhydrous tetramethylammonium chloride in sulfolane T=180°C; 6 h; effect of other nitrite ion traps; other substrates; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 56, # 22 p. 6406 - 6411
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in sulfolane T=180°C;
参考文献
Journal of Organic Chemistry, , vol. 56, # 22 p. 6406 - 6411
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in sulfolane T=130°C; 3 h;
参考文献
Maggini, Michele; Passudetti, Margherita; Gonzales-Trueba, Guadalupe; Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Journal of Organic Chemistry, 1991 , vol. 56, # 22 p. 6406 - 6411
反应条件
potassium fluoride; water; N,N-dimethyl-formamide T=160°C;
参考文献
Finger; Kruse
Journal of the American Chemical Society, 1956 , vol. 78, p. 6034,6037
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in sulfolane T=180°C;
参考文献
Maggini, Michele; Passudetti, Margherita; Gonzales-Trueba, Guadalupe; Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Journal of Organic Chemistry, 1991 , vol. 56, # 22 p. 6406 - 6411
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in sulfolane T=180°C;
参考文献
Maggini, Michele; Passudetti, Margherita; Gonzales-Trueba, Guadalupe; Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Journal of Organic Chemistry, 1991 , vol. 56, # 22 p. 6406 - 6411
反应条件
copper(I) bromide; lithium bromide in tetrahydrofuran T=160°C; 6 h; Product distribution / selectivity;
参考文献
Bayer CropScience S.A.
Patent: US6635780 B1, 2003 ;
Location in patent: Page/Page column 12 ;
