2-甲基-5-硝基苯磺酰氯合成路线 （共 11 条）
参考文献
Tagiev; Kazaz; Anyl
Russian Journal of Applied Chemistry, 2012 , vol. 85, # 10 p. 1581 - 1585
Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.), 2012 , vol. 85, # 10 p. 1648 - 1652,5
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 117, p. 21
反应条件
Erhitzen unter vermindertem Druck;
参考文献
Bulmer; Mann
Journal of the Chemical Society, 1945 , p. 666,671
反应条件
1: conc. aq. NH3 / diethyl ether / 2 h / Heating 2: 56 percent / CrO3, conc. H2SO4 / H2O / 24 h / Ambient temperature 3: 63 percent / cyclohexene / 5percent Pd/C / ethanol / 2 h / Heating View Scheme
参考文献
Gener, Nahit; Demir, Dudu; Sonmez, Fatih; Kucukislamoglu, Mustafa
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 9 p. 2811 - 2821
反应条件
ammonium hydroxide in diethyl ether T=0°C; 42 h; Inert atmosphere;
参考文献
ABBOTT LABORATORIES; CALDERWOOD, David, J.; WILSON, Noel, S.; COX, Philip; HOEMANN, Michael, Z.; CLAPHAM, Bruce; MULLEN, Kelly, D.; VASUDEVAN, Anil; VILLAMIL, Clara I; LI, Bin; SOMAL, Gagandeep
Patent: WO2012/48222 A1, 2012 ;
Location in patent: Page/Page column 98 ;
WO 2012/048222 A1
反应条件
pyridine in 1,4-dioxane
参考文献
American Home Products Corporation
Patent: US6355633 B1, 2002 ;
反应条件
1: conc. aq. NH3 / diethyl ether / 2 h / Heating 2: 56 percent / CrO3, conc. H2SO4 / H2O / 24 h / Ambient temperature View Scheme
参考文献
Sonmez, Fatih; Bilen, Cigdem; Sumersan, Sinem; Gencer, Nahit; Isik, Semra; Arslan, Oktay; Kucukislamoglu, Mustafa
Journal of Enzyme Inhibition and Medicinal Chemistry, 2014 , vol. 29, # 1 p. 118 - 123
反应条件
nachfolgend Reduktion;
参考文献
Bayer and Co.
Patent: DE282889 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 327
参考文献
Green; Marsden; Scholefield
Journal of the Chemical Society, 1904 , vol. 85, p. 1436
参考文献
Ullmann; Gschwind
Chemische Berichte, 1908 , vol. 41, p. 2296
