4-乙氧羰基苯基硫代异氰酸酯合成路线 (共 11 条)
反应条件
triethylamine in tetrahydrofuran T=25°C; 12 h;
参考文献
Wilcox, Craig S.; Kim, Eun-il; Romano, David; Kuo, Lung Huang; Burt, Arthur L.; Curran, Dennis P.
Tetrahedron, 1995 , vol. 51, # 2 p. 621 - 634
反应条件
in dichloromethane T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Witek, Rachel M.; Rodriguez-Garcia, Valerie; Mohapatra, Prabhu P.; Rogers, James W.; Cusido, Janet; Abdel-Fattah, Ashraf A. A.; Steel, Peter J.
Journal of Organic Chemistry, 2005 , vol. 70, # 20 p. 7866 - 7881
反应条件
1: acetone / 20 °C 2: bis(trichloromethyl) carbonate / chloroform / 4.5 h / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 43, # 24 p. 3342 - 3351
反应条件
1: 4-amino-benzoic acid ethyl ester With 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide T=20°C; 12 h; 2: bis(trichloromethyl) carbonate Reflux;
参考文献
Chemical Biology and Drug Design, , vol. 76, # 1 p. 25 - 33
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 12 p. 3916 - 3920
反应条件
1.1: thionyl chloride / 4 h / Reflux 1.2: pH 7 - 8 2.1: 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide / 12 h / 20 °C 2.2: Reflux View Scheme
参考文献
Chemical Biology and Drug Design, , vol. 76, # 1 p. 25 - 33
参考文献
Journal of the Chemical Society, , p. 440
参考文献
Hunter; Parken
Journal of the Indian Chemical Society, 1932 , vol. 9, p. 357,359
参考文献
Klayman; Bartosevich; Griffin; Mason; Scovill
Journal of Medicinal Chemistry, 1979 , vol. 22, # 7 p. 855 - 862
参考文献
Dyson; George; Hunter
Journal of the Chemical Society, 1927 , p. 440