反应条件
in water High Pressure; stoich. amt. of salts were dissolved in the solvent, thioglycolic acid was added dropwise under stirring, 2 equiv. of thiourea was added, stirring for 30 min, teflon-lined autoclave, 160 °C for 20 h; cooling to room temp., ppt. was filtered off, washed with H2O and abs. EtOH several times, dried in vac. at 60 °C for 4 h;
参考文献
Chemistry Letters, , vol. 35, # 9 p. 1050 - 1051
