3 - (二甲氨基)- 1 -苯基 -2-丙烯-1-酮合成路线 (共 43 条)
参考文献
Masson, Christophe; Caumont-Bertrand, Karine
Patent: US2011/195993 A1, 2011 ;
Location in patent: Page/Page column 10; 14 ;
US 20110195993 A1
反应条件
methanol; sodium in 1,4-dioxane 3 h; Reflux;
参考文献
Saleh, Tamer S.; Al-Omar, Mohamed A.; Abdel-Aziz, Hatem A.
Letters in Organic Chemistry, 2010 , vol. 7, # 6 p. 483 - 486
反应条件
in benzene 15 h; Ambient temperature;
参考文献
Nishio, Takehiko; Omote, Yoshimori
Synthesis, 1980 , # 5 p. 390 - 392
反应条件
1: 70 percent / 3-Chlorobenzenecarboperoxoic acid / CHCl3 / 1.) ice-bath, 2.) r.t., 15 h 2: 90 percent / benzene / 15 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 5 p. 390 - 392
反应条件
in ethyl acetate 16 h; Ambient temperature;
参考文献
Kantlehner, Willi; Hauber, Michael
Bulletin des Societes Chimiques Belges, 1994 , vol. 103, # 12 p. 697 - 704
反应条件
in N,N-dimethyl acetamide T=110 - 125°C; 24 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 12 p. 3821 - 3825
反应条件
sodium amide in ammonia
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 25, p. 1302 - 1307
反应条件
in benzene 0.5 h; Ambient temperatureIrradiation;
参考文献
Nishio, Takehiko; Nakajima, Naoko; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 405 - 406
反应条件
1: diethyl ether 2: H2O View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1704 - 1710
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 1764 - 1772
反应条件
1: NaOEt / diethyl ether 2: Na2SO4 / diethyl ether View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2328 - 2332