3,4,5-三氯-2-(三氯甲基)吡啶合成路线 （共 14 条）
反应条件
ammonia T=100°C; 1 h;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
hydrogenchloride; chlorine T=105 - 110°C;
参考文献
McBee et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 389
反应条件
chlorine T=150°C; 2 h; Irradiationother temp.: 80, 90, 100, 120 deg. C; other reaction time: 2 to 45 h; reaction without irradiation; reaction in C4Cl6; Product distributionKinetics;
参考文献
Kosorotov, V. I.; Stul', B. Ya.; Dzhagatspanyan, R. B.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1845 - 1851
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2163 - 2171
参考文献
Sell
Journal of the Chemical Society, 1905 , vol. 87, p. 801
Journal of the Chemical Society, 1908 , vol. 93, p. 1993
参考文献
Ochiai; Okuda
Yakugaku Zasshi, 1950 , vol. 70, p. 156,159
Chem.Abstr., 1950 , p. 5878
Full Text Show Details
McBee et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 389
反应条件
ammonia in dimethyl sulfoxide T=100°C; 22 h;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
1: sulfuric acid / 120 - 130 °C 2: hydrogen chloride 3: aqueous methanol; ammonia View Scheme
参考文献
Sell
Journal of the Chemical Society, 1905 , vol. 87, p. 801
Journal of the Chemical Society, 1908 , vol. 93, p. 1993
反应条件
chlorine T=200°C; 18 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 6 p. 1168 - 1171
Zhurnal Organicheskoi Khimii, , vol. 19, # 6 p. 1308 - 1312
参考文献
Kalama Chemical, Inc.
Patent: US4517369 A1, 1985 ;
反应条件
chlorine T=200°C; 18 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 6 p. 1168 - 1171
Zhurnal Organicheskoi Khimii, , vol. 19, # 6 p. 1308 - 1312
