N,N-二乙基-4-氨基苯甲醛合成路线 (共 64 条)
反应条件
formic acid; ethanol; acetic acid
参考文献
Journal of the Chemical Society, , p. 276
参考文献
Chemische Berichte, , vol. 37, p. 862
反应条件
potassium hydroxide; sodium hydroxide
参考文献
Ott et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5448,5452
反应条件
ammonium acetate in nitromethane
参考文献
NIPPON TELEGRAPH AND TELEPHONE CORPORATION
Patent: EP326133 A2, 1989 ;
参考文献
Forman, Barry; Yu, Donna
Patent: US2006/189825 A1, 2006 ;
Location in patent: Page/Page column 7; 12; Sheet 3/7 ;
US 20060189825 A1
反应条件
1: 76 percent / AcOH / ethanol / Heating 2: K2CO3 3: BBr3 View Scheme
参考文献
Yu, Donna D.; Forman, Barry Marc
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 5 p. 1311 - 1313
参考文献
Zuercher, William J.; Gaillard, Stephanie; Orband-Miller, Lisa A.; Chao, Esther Y. H.; Shearer, Barry G.; Jones, David G.; Miller, Aaron B.; Collins, Jon L.; McDonnell, Donald P.; Willson, Timothy M.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 9 p. 3107 - 3109
反应条件
1: 1.) Zn, PPh3 / 1.) CH2Cl2, 2 h, 2.) overnight 2: 83.9 percent / n-BuLi / hexane; tetrahydrofuran / 1.) -78 deg C, 45 min, 2.) r.t., 1 h View Scheme
参考文献
UNIVERSITAeT POTSDAM; AST, Sandra; HOLDT, Hans-Juergen
Patent: WO2012/120141 A1, 2012 ;
反应条件
1: 4-Methylpyridine With sodium hydride in N,N-dimethyl-formamide T=60°C; 2 h; Inert atmosphere; 2: 4-[N,N-bis(ethyl)amino]benzaldehyde T=60°C; 7 h; Inert atmosphere;
参考文献
Lacroix, Pascal G.; Munoz, M. Carmen; Gaspar, Ana Belen; Real, Jose Antonio; Bonhommeau, Sebastien; Rodriguez, Vincent; Nakatani, Keitaro
Journal of Materials Chemistry, 2011 , vol. 21, # 40 p. 15940 - 15949
反应条件
piperidine; acetic acid; toluene
参考文献
Parker; Furst
Journal of Organic Chemistry, 1958 , vol. 23, p. 201