119072-55-8合成路线 （共 225 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene 2 h; Inert atmosphereReflux;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
反应条件
1: tert-butylisonitrile; 2-amino-5-methoxy-benzenethiol; hydrochloride in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere; 2: iodobenzene With 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
参考文献
Yamamoto,Y. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 3682 - 3685
Full Text Show Details
Yamamoto,Y. et al.
Tetrahedron Letters, 1974 , p. 793 - 796
反应条件
(i) , (ii) /BRN= 3029741/, (iii) NaOH, aq. H2O2; Multistep reaction;
参考文献
Yamamoto,Y. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 3682 - 3685
反应条件
1: tert-butylisonitrile; phenylacetylene With Ti(NMe2)2(dpma); cyclohexylamine in toluene T=100°C; 24 h; Inert atmosphere; 2: methanimidamide monoacetate in 1,1-dimethylpropan-1-ol T=140°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 66, # 17 p. 3152 - 3158
反应条件
palladium diacetate; cupric trifluoroacetate in 1,2-dichloro-ethane T=70°C; 1 h; Sealed tube;
参考文献
Peng, Jiangling; Zhao, Jiaji; Hu, Ziwei; Liang, Dongdong; Huang, Jinbo; Zhu, Qiang
Organic Letters, 2012 , vol. 14, # 18 p. 4966 - 4969,4
反应条件
aluminium trichloride in dichloromethane 7 h; Ambient temperature;
参考文献
Ito, Yoshihiko; Kato, Hidehito; Imai, Hiroshi; Saegusa, Takeo
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6449 - 6450
参考文献
Saegusa,T. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 12 p. 4040 - 4046
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux; Catalytic behavior; Reagent/catalystSolvent;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
