4,4'-二氨基-3,3'-二甲基联苯合成路线 (共 34 条)
反应条件
1: 99 percent / P(t-Bu)3*HBF4; Cs2CO3; Pd(OAc)2 / toluene / 2 h / Heating 2: 81 percent / hydrochloric acid / ethanol / 2 h / 80 °C View Scheme
参考文献
Organic Letters, , vol. 8, # 10 p. 2047 - 2050
反应条件
sodium carbonate; palladium; isopropyl alcohol T=80°C; P=7355.08 Torr; anschliessend Behandeln mit wss.Salzsaeure und mit Eisen;
反应条件
lithium aluminium tetrahydride in diethyl ether Reduction; 24 h; Heating;
参考文献
You; Brezzell; Das; Espadas-Torre; Hooberman; Sinsheimer
Mutation Research - Genetic Toxicology Testing and Biomonitoring of Environmental or Occupational Exposure, 1993 , vol. 319, # 1 p. 19 - 30
反应条件
ethanol; tin(ll) chloride
参考文献
Chemische Berichte, , vol. 17, p. 467
反应条件
1: 22 percent / conc. H2SO4 / 48 h / Heating 2: 24 percent / LiAlH4 / diethyl ether / 24 h / Heating View Scheme
参考文献
Mutation Research - Genetic Toxicology Testing and Biomonitoring of Environmental or Occupational Exposure, , vol. 319, # 1 p. 19 - 30
反应条件
hydrogenchloride; sodium hydrogensulfite; xylene
参考文献
J.Sci.Ind.Res.India, , vol. 4, p. 637,640
反应条件
sulfuric acid bei der elektrolytischen Reduktion, an Kohlenstoffanode und Platinkathode;
参考文献
Chemiker-Zeitung, Chemische Apparatur, , vol. 17, p. 209
反应条件
sodium tetrathionate in various solvent(s) T=70°C; Reduction; pH=6; Product distribution; Further Variations:Reaction partners;
参考文献
Human and Experimental Toxicology, , vol. 18, # 9 p. 552 - 559
反应条件
in N,N-dimethyl-formamide 3 h; Electrolysis;
参考文献
Journal of the Indian Chemical Society, , vol. 87, # 9 p. 1117 - 1123
反应条件
hydrogenchloride; acetic acid; tin(ll) chloride 2 h; Title compound not separated from byproducts;
参考文献
Polish Journal of Chemistry, , vol. 58, # 10-12 p. 1035 - 1045