2, 2'-二硫代二苯甲酸合成路线 （共 163 条）
反应条件
XeF2 in dichloromethane T=25°C;
参考文献
Ghorbani-Choghamarani, Arash; Azadi, Gouhar; Tahmasbi, Bahman; Hadizadeh-Hafshejani, Mojtaba; Abdi, Zainab
Phosphorus, Sulfur and Silicon and the Related Elements, 2014 , vol. 189, # 4 p. 433 - 439
参考文献
12 <New York 1932>, S. 76
反应条件
1: 2-mercapto benzoic acid With sodium hydride in N,N-dimethyl-formamide T=20°C; Inert atmosphere; 2: perfluoromethyl iodide in N,N-dimethyl-formamide T=20°C; 14 h; 3: With hydrogenchloride in water; N,N-dimethyl-formamide T=20°C;
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 12 p. 1241 - 1246
反应条件
sodium sulfide; sodium hydroxide; sulfur in water T=5 - 60°C; 4 h;
参考文献
US2004/116734 A1, ;
Page 3 ;
反应条件
copper(l) iodide; tetra(n-butyl)ammonium hydroxide; sulfur in water T=80°C; 48 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2296 - 2300
反应条件
n-butyllithium 1.) hexane, r.t., overnight, 2.) r.t.; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 111, p. 665
反应条件
1: 71 percent / 3-chloroperbenzoic acid / acetone 2: dimethylsulfoxide-d6 / 10 h / 110 °C View Scheme
参考文献
Chemische Berichte, , vol. 116, # 5 p. 1708 - 1727
反应条件
in dimethylsulfoxide-d6 T=110°C; 10 h;
参考文献
Chemische Berichte, , vol. 116, # 5 p. 1708 - 1727
参考文献
Journal of the Indian Chemical Society, , vol. 6, p. 276
Chem. Zentralbl., , vol. 100, # II p. 1004
DE205450 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 9, p. 541
Organic Syntheses, , vol. 12, p. 78; Coll. Vol. II <1943>, 582
反应条件
1: 1) n-BuLi, anhydr. TMEDA, 2) MeOH / 1) r.t, 12h, 2) 0 deg C 2: 1) n-butyllithium, 2) aq. HCl View Scheme
参考文献
Tetrahedron, , vol. 46, # 3 p. 861 - 884
