5-溴-1-苯基磺酰-1H-吲哚合成路线 （共 4 条）
反应条件
1: 5-Bromo-1H-indole With sodium hydride in tetrahydrofuran T=0 - 20°C; 2: benzenesulfonyl chloride in tetrahydrofuran T=0 - 50°C;
参考文献
H. LUNDBECK A/S; ESKILDSEN, Jørgen
Patent: WO2014/49133 A1, 2014 ;
Location in patent: Page/Page column 31 ;
反应条件
manganese triacetate in acetic acid T=110°C;
参考文献
Ketcha, Daniel M.
Tetrahedron Letters, 1988 , vol. 29, # 18 p. 2151 - 2154
反应条件
benzenesulfonyl chloride in sodium hydroxide; toluene
反应条件
sodium t-butanolate in 1,4-dioxane T=80°C; 3 h; Inert atmosphere;
参考文献
Chaulet, Charlotte; Croix, Cecile; Basset, Joan; Pujol, Maria-Dolores; Viaud-Massuard, Marie-Claude
Synlett, 2010 , # 10 p. 1481 - 1484
