1165952-92-0合成路线 (共 138 条)
反应条件
1: 35 percent / m-chloroperbenzoic acid 2: 73 percent / LiAlH4 3: 65 percent View Scheme
参考文献
Lambert, Joseph B.; Marko, Dale E.
Journal of the American Chemical Society, 1985 , vol. 107, # 26 p. 7978 - 7982
反应条件
in ethanol mixt. of Ru compd. and diene (11 equiv.) in ethanol was refluxed for 12 h; cooled; filtered under suction; washed (methanol);
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 3 p. 416 - 427
反应条件
in ethanol; water Ru salt refluxed in degassed aq. EtOH with excess of diene under N2 for5-10 min;
参考文献
Journal of Organometallic Chemistry, , vol. 208, # 3 p. 369 - 387
反应条件
ammonia; acetic acid; Pd on carbon in methanol; ethanol; 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
Bryant, Helen Jane; Chambers, Mark Stuart; Jones, Philip; MacLeod, Angus Murray; Maxey, Robert James
Patent: US2003/125333 A1, 2003 ;
参考文献
Cornubert; Rio; Senechal
Bulletin de la Societe Chimique de France, 1955 , p. 46,50
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Sakashita
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 972,973
Chem.Abstr., 1960 , p. 2008
反应条件
1: 63 percent / tetraphenylporphyrin; O2 / CH2Cl2 / 48 h / 20 °C / Photolysis 2: 95 percent / Me2S; Ti(Oi-Pr)4 / CH2Cl2; diethyl ether / 5 °C 3: Candida cylindracea lipase VII / 38 h / 20 °C 4: thiourea 5: OsO4; NMO 6: NH3 / methanol View Scheme
参考文献
Gueltekin, M. Serdar; Celik, Murat; Turkut, Engin; Tanyeli, Cihangir; Balci, Metin
Tetrahedron Asymmetry, 2004 , vol. 15, # 3 p. 453 - 456
反应条件
in tetrachloromethane T=30°C; other solvents; Rate constant;
参考文献
Valgimigli, Luca; Ingold; Lusztyk
Journal of Organic Chemistry, 1996 , vol. 61, # 22 p. 7947 - 7950
反应条件
Nitrous oxide T=250°C; 5 h; pressure;
参考文献
Starokon; Dubkov; Babushkin; Parmon; Panov
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 268 - 274
反应条件
1: T=80°C; 4 h; 2: With sodium hydroxide in dichloromethane; water T=20°C;
参考文献
Lee, Myung-Ryul; Stahl, Shannon S.; Gellman, Samuel
Organic Letters, 2008 , vol. 10, # 22 p. 5317 - 5319
反应条件
1: toluene / 13 h / 0 - 20 °C 2: aq. Na2SO3 View Scheme
参考文献
Nivsarkar, Manisha; Thavaselvam; Prasanna; Sharma, Mamta; Kaushik
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 5 p. 1371 - 1373