1165952-91-9合成路线 （共 295 条）
反应条件
1.1: Ni(cod)2; DBU / tetrahydrofuran / 7 h / 0 °C / 760.05 Torr 1.2: 50 percent / Me2Zn / tetrahydrofuran / 2 h / 0 °C 2.1: diethyl ether / 0 °C 2.2: 100 percent / H2 / Pd/C / ethyl acetate / 20 °C View Scheme
参考文献
Takimoto; Mori
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2895 - 2896
参考文献
Cornubert; Rio; Senechal
Bulletin de la Societe Chimique de France, 1955 , p. 46,50
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Sakashita
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 972,973
Chem.Abstr., 1960 , p. 2008
反应条件
dimethylsulfide; ozone 1.) methylene chloride, -78 deg C, 10 min; 2.) methylene chloride, 0 deg C, overnight; Yield given. Multistep reaction;
参考文献
Hudlicky; Luna; Barbieri; Kwart
Journal of the American Chemical Society, 1988 , vol. 110, # 14 p. 4735 - 4741
反应条件
sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide other cyclic dienes and hydroborating agents; Product distribution;
参考文献
Brown, Herbert C.; Bhat, Krishna S.
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 445 - 449
反应条件
1: Diels-Alder reaction; 2: With silver(l) oxide 3: Heating;
参考文献
Koyama, Junko; Morita, Izumi; Kobayashi, Norihiro; Osakai, Toshiyuki; Usuki, Yoshinosuke; Taniguchi, Makoto
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 4 p. 1079 - 1082
反应条件
1: (heating) 2: NaBH4 3: (i) Na, (ii) CS2, MeI, (iii) (pyrolysis) View Scheme
参考文献
Belikova,N.A. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, p. 1759 - 1764
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 9 p. 1898 - 1903
反应条件
(i) , (ii) NaOH, ethane-1,2-diol; Multistep reaction;
参考文献
Davies,D.I.; Parfitt,L.T.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1401 - 1408
反应条件
hydroquinone T=120°C; 40 h; Further byproducts given;
参考文献
Lucchi, Ottorino De; Piccolrovazzi, Nicoletta; Licini, Giulia; Modena, Giorgio; Valle, Giovanni
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 401 - 408
参考文献
Lucchi, Ottorino De; Piccolrovazzi, Nicoletta; Licini, Giulia; Modena, Giorgio; Valle, Giovanni
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 401 - 408
反应条件
1: carbon dioxide; cyclohexa-1,3-diene With bis(1,5-cyclooctadiene)nickel (0); 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=0°C; P=760.051 Torr; 7 h; 2: carbon dioxide With dimethyl zinc in tetrahydrofuran T=0°C; 2 h; Further stages.;
参考文献
Takimoto; Mori
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2895 - 2896
