2,6-二甲基-4-苯基-1,4-二氢吡啶-3,5-二羧酸二乙酯合成路线 (共 49 条)
反应条件
sodium nitrate; sulfuric acid 1) 0 to -8 deg C, 15 min; 2) 30 min; Yield given;
参考文献
Tirzit, G. D.; Skrastin'sh, I. P.; Dubur, G. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 1 p. 55 - 56
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 1 p. 68 - 69
反应条件
N-bromosuccinmide in methanol T=20°C; 0.0833333 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 45, # 3 p. 826 - 828
反应条件
bei der trocknen Destillation;
参考文献
Chem. Zentralbl., , vol. 70, # II p. 440
反应条件
ammonium cerium(IV) nitrate in water; acetone 0.166667 h; Ambient temperature;
参考文献
Heravi, Majid M.; Derikvand, Fatemeh; Oskooie, Hossein A.; Hekmatshoar, Rahim
Journal of Chemical Research, 2006 , # 3 p. 168 - 169
反应条件
N-bromosuccinmide in methanol T=20°C; 0.0833333 h;
参考文献
Nagarajan; Anthonyraj; Muralidharan; Saikumar; Perumal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 826 - 828
反应条件
Sodium bromate; ammonium cerium(IV) nitrate in water; acetonitrile T=80°C; 6 h;
参考文献
Pfister
Synthesis, 1990 , # 8 p. 689 - 690
反应条件
anhydrous potassium sulfate; potassium hydrogensulfate; oxone in acetonitrile 0.166667 h; Heating;
参考文献
Liu, Zhengang; Yu, Wei; Yang, Li; Liu, Zhong-Li
Tetrahedron Letters, 2007 , vol. 48, # 30 p. 5321 - 5324
反应条件
ammonium acetate in neat (no solvent)
T=60°C; Green chemistry;
参考文献
Rostamnia, Sadegh; Pourhassan, Fatemeh
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 401 - 403
反应条件
1: With cellulose sulfuric acid in neat (no solvent)
T=80 - 100°C; Hantzsch Pyridine Synthesis;
2: With cellulose sulfuric acid in neat (no solvent)
Hantzsch Pyridine Synthesis;
参考文献
Murthy; Rajack, Abdul; Taraka Ramji; Jeson Babu; Praveen, Ch.; Aruna Lakshmi
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 18 p. 6016 - 6023
反应条件
ammonia
3 h; Heating;
参考文献
Rimoli, Maria Grazia; Avallone, Lucia; Zanarone, Serena; Abignente, Enrico; Mangoni, Alfonso
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1117 - 1122