1: (+/-)-Phenyl-1,2-ethanediol With peracetic acid; C9H17NO5S(1-)*C11H12IN2(1+); acetic acid in hexafluoroisopropyl alcohol T=20°C; 8 h; 2: (2,4-dinitro-phenyl)-hydrazine With sulfuric acid in diethyl ether; ethanol; water
参考文献
Zhu, Chenjie; Yoshimura, Akira; Wei, Yunyang; Nemykin, Victor N.; Zhdankin, Viktor V.
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1438 - 1444
1: benzyl alcohol With peracetic acid; C9H17NO5S(1-)*C11H12IN2(1+); acetic acid in hexafluoroisopropyl alcohol T=20°C; 8 h; 2: (2,4-dinitro-phenyl)-hydrazine With sulfuric acid in diethyl ether; ethanol; water
1: phenylacetaldehyde With tetrafluoroboric acid; iodosylbenzene in 1,4-dioxane; water T=20°C; 144 h; 2: (2,4-dinitro-phenyl)-hydrazine With sulfuric acid in 1,4-dioxane; water
参考文献
Havare, Nizam; Plattner, Dietmar A.
Organic Letters, 2012 , vol. 14, # 19 p. 5078 - 5081,4
in tetrahydrofuran soln. of complex in THF was refluxed for 6 days, cooled to room temp. (N2 atm.); cooled at -20°C for 2 h; ppt. was filtered, C6H5CHO was in the filtrate;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 1455
