1: 2-mercaptobenzoimidazole With sodium hydride in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
2: perfluoromethyl iodide in N,N-dimethyl-formamide
T=20°C; 14 h;
3: With hydrogenchloride in water; N,N-dimethyl-formamide
T=20°C;
sodium hydroxide in water; acetone
18 h; Ambient temperature;
参考文献
Griffiths, David; Hull, Roy; Seden, Timothy P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2608 - 2612