2-甲基-3-丁烯-2-醇合成路线 (共 471 条)
反应条件
hydrogen in water T=45°C; P=760 Torr; 10 h; <Me2C(OH)CCH>/<Co> : 2; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 12 p. 1915 - 1918
参考文献
BASF Aktiengesellschaft
Patent: US4645863 A1, 1987 ;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 240, p. 314
参考文献
Chemistry and Industry (London, United Kingdom), , p. 402
Journal of the American Chemical Society, , vol. 84, p. 361,363
Journal of the American Chemical Society, , vol. 84, p. 361,363
反应条件
1: NaBH4 / ethanol / 2 h / 15 - 20 °C 2: H2O2 / 2 h / 15 - 20 °C / var. oxidants and time. View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 7 p. 921 - 924
反应条件
sodium hydrogencarbonate T=45°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 18, p. 419,421
Chem.Abstr., , p. 114
反应条件
sodium in ammonia Yield given;
参考文献
Tetrahedron Letters, , vol. 25, # 5 p. 527 - 528
反应条件
1: With tert.-butylhydroperoxide; Al tri-t-BuO- in benzene T=20°C; 24 h; 2: With sulfuric acid in diethyl ether Further byproducts given. Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 71, # 5 p. 736 - 741
反应条件
1: 82 percent / NBS 2: t-BuOK, 18-couronne-6 / benzene / Heating 3: Na / liquid ammonia View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 5 p. 527 - 528