N-苄氧羰基-L-丝氨酸合成路线 (共 73 条)
反应条件
dichloromethane; dicyclohexyl-carbodiimide
参考文献
Koenig,W.; Geiger,R.
Chemische Berichte, 1970 , vol. 103, p. 788 - 798
反应条件
dicyclohexyl-carbodiimide
参考文献
Fujino,M.; Nishimura,O.
Chemical and Pharmaceutical Bulletin, 1969 , vol. 17, p. 1937 - 1941
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=-78°C;
参考文献
Ross, Fiona C.; Botting, Nigel P.; Leeson, Paul D.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 22 p. 2643 - 2646
反应条件
triphenylphosphine in acetonitrile
参考文献
Aventis Pharma Deutschland GmbH
Patent: US2003/119820 A1, 2003 ;
US 20030119820 A1
反应条件
triphenylphosphine; diethylazodicarboxylate in acetonitrile T=-35 - 5°C; 12 h;
参考文献
AVENTIS PHARMA DEUTSCHLAND GMBH
Patent: WO2004/22553 A1, 2004 ;
Location in patent: Page/Page column 12-13 ;
WO 2004/022553 A1
反应条件
camphor-10-sulfonic acid in benzene cyclocondensation; Heating;
参考文献
Australian Journal of Chemistry, , vol. 53, # 5 p. 425 - 433
反应条件
MeO2CN=NCO2Me; triphenylphosphine in tetrahydrofuran T=20°C;
参考文献
Ramer, Shawn E.; Moore, Richard N.; Vederas, John C.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 706 - 713
反应条件
1: 1.)isobutyl chloroformate, N-methylmorpholine; 2.)triethylamine / 1.) THF, -15 deg C, 5 min; 2.) THF, -15 deg C, 1h 2: t-butyl thiol / tetrahydrofuran / Ambient temperature; Irradiation View Scheme
参考文献
Barton, Derek H. R.; Herve, Yolande; Potier, Pierre; Thierry, Josiane
Tetrahedron, 1988 , vol. 44, # 17 p. 5479 - 5486
反应条件
palladium/alumina; hydrogen T=70°C; neat (no solvent);
参考文献
Beilstein Journal of Organic Chemistry, , vol. 7, art. no. 83, p. 735 - 739
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in benzene
参考文献
Bhat, Ramakrishna G.; Porhiel, Emmanuel; Saravanan, Vadivelu; Chandrasekaran, Srinivasan
Tetrahedron Letters, 2003 , vol. 44, # 28 p. 5251 - 5253