2-(2-甲氧基乙基)吡啶合成路线 （共 8 条）
反应条件
Co(2-ethylhexanoate)2-Al(C2H5)2; cobalt(II) 2-ethylhexanoate in toluene T=150°C; P=9880 Torr; 10 h; Yield given. Yields of byproduct given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 3 p. 290 - 295
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 20, # 3 p. 360 - 365
反应条件
Brij 56; cyclopentadienyl-cyclooctadienyl-cobalt(I) in water 4 h; Ambient temperatureIrradiation;
参考文献
Heller, Barbara; Oehme, Guenther
Journal of the Chemical Society, Chemical Communications, 1995 , # 2 p. 179 - 180
反应条件
mercury(II) trifluoroacetate 1.) 10 min, 2.) irrad., 40 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 50, # 18 p. 3423 - 3425
反应条件
hydrogenchloride 2 h; Ambient temperatureIrradiationother alcohols; other acids; effect of hydrochloric acid; var. conditions; Product distribution;
参考文献
Ishida, Akito; Uesugi, Tatsumi; Takamuku, Setsuo
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 5 p. 1580 - 1582
反应条件
triphenyl boroxine; triphenyl phosphite; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2
参考文献
Ogiwara, Yohei; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2011 , vol. 13, # 12 p. 3254 - 3257
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in ethanol P=3345.86 Torr; 15 h; Parr shaker;
参考文献
PFIZER INC.; CAMERON, Kimberly O'Keefe; PERRY, David Austen
Patent: WO2010/67233 A1, 2010 ;
Location in patent: Page/Page column 60 ;
WO 2010/067233 A1
反应条件
triphenyl phosphite; methanol; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene
T=120°C; 24 h;
参考文献
Ogiwara, Yohei; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2011 , vol. 13, # 12 p. 3254 - 3257
反应条件
1: triphenyl boroxine; triphenyl phosphite; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2
2: triphenyl phosphite; methanol; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2
View Scheme
参考文献
Ogiwara, Yohei; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2011 , vol. 13, # 12 p. 3254 - 3257
