(反式)-1,1'-(1,2-环丙烷二基)二苯合成路线 （共 61 条）
反应条件
C3H6C9H10N4 in N,N-dimethyl-formamide T=20°C; 90 h; Inert atmosphereUV-irradiation;
参考文献
Cahard, Elise; Schoenebeck, Franziska; Garnier, Jean; Cutulic, Sylvain P. Y.; Zhou, Shengze; Murphy, John A.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3673 - 3676
反应条件
potassium-sodium in tetrahydrofuran T=0°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 25, # 28 p. 2961 - 2964
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide T=20°C; 90 h; Inert atmosphereUV-irradiation;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 15 p. 3673 - 3676
参考文献
Kasansski; Lukina; Safomowa
Doklady Akademii Nauk SSSR, 1960 , vol. 130, p. 322
Doklady Chemistry, 1960 , vol. 130, p. 55
反应条件
T=0°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tomioka, Hideo; Ozaki, Yasuji; Koyabu, Yasuhiro; Izawa, Yasuji
Tetrahedron Letters, 1982 , vol. 23, # 18 p. 1917 - 1920
反应条件
potassium fluoride; sodium bromide; tetrakis(triphenylphosphine) palladium(0) in toluene
T=100°C; Phenylation;
参考文献
Yao, Min-Liang; Deng, Min-Zhi
Synthesis, 2000 , # 8 p. 1095 - 1100
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in hexane; dichloromethane
0.333333 h; cooling;
2: meso-1,2-diphenylethylene in hexane; dichloromethane
T=20°C; 1 h;
参考文献
Lorenz, Jon C.; Long, Jiang; Yang, Zhiqiang; Xue, Song; Xie, Yinong; Shi, Yian
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 327 - 334
反应条件
1: (+/-)-di-tert-butoxy((1S,2R)-2-phenylcyclopropyl)silanol With boron trifluoride diethyl etherate
0.25 h; Inert atmosphere;
2: bromobenzene With tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran
T=100°C; Hiyama-Denmark cross-coupling; 17 h; Inert atmosphere;
参考文献
Beaulieu, Louis-Philippe B.; Delvos, Lukas B.; Charette, Andre B.
Organic Letters, 2010 , vol. 12, # 6 p. 1348 - 1351
反应条件
diethylzinc in dichloromethane-d2
T=20°C; Irradiation;
参考文献
Charette; Beauchemin; Francoeur
Journal of the American Chemical Society, 2001 , vol. 123, # 33 p. 8139 - 8140
反应条件
copper(l) iodide; lithium chloride; palladium diacetate in N,N-dimethyl-formamide
T=80°C; de Meijere reaction;
参考文献
Heureux, Nicolas; Marchant, Melanie; Maulide, Nuno; Berthon-Gelloz, Guillaume; Hermans, Christophe; Hermant, Sebastien; Kiss, Eleonora; Leroy, Bernard; Wasnaire, Pierre; Marko, Istvan E.
Tetrahedron Letters, 2005 , vol. 46, # 1 p. 79 - 83
