3-(叔丁基二甲基硅氧基)戊二酸合成路线 （共 4 条）
反应条件
acetic anhydride T=130 - 135°C; 2 - 3 h;
参考文献
TEVA PHARMACEUTICAL INDUSTRIES LTD.; TEVA PHARMACEUTICALS USA, INC.
Patent: WO2008/130638 A2, 2008 ;
Location in patent: Page/Page column 30-31 ;
反应条件
Novozym 435 in 2,2,4-trimethylpentane T=35°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bo; Liu, Ji; Tang, Xiaoling; Cheng, Cheng; Gu, Jiali; Dai, Liyan; Yu, Hongwei
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 309 - 312
反应条件
Novozym 435 in toluene T=35°C; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bo; Liu, Ji; Tang, Xiaoling; Cheng, Cheng; Gu, Jiali; Dai, Liyan; Yu, Hongwei
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 309 - 312
反应条件
Novozym 435 in 2,2,4-trimethylpentane
T=35°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bo; Liu, Ji; Tang, Xiaoling; Cheng, Cheng; Gu, Jiali; Dai, Liyan; Yu, Hongwei
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 309 - 312
