4,4'-二甲基-2,2'-联吡啶合成路线 （共 79 条）
反应条件
water in acetonitrile T=20°C;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 72 - 81
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water T=80 - 90°C; Suzuki cross-coupling reaction; 16 h;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 22 p. 4809 - 4827
反应条件
water in acetonitrile T=20°C;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 72 - 81
反应条件
water in acetonitrile T=30°C;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 72 - 81
反应条件
n-butyllithium; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 22, p. 939,942
Journal of the American Chemical Society, , vol. 70, p. 2809
Chemische Berichte, , vol. 89, p. 712
反应条件
in methanol T=20°C; 24 h;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 72 - 81
反应条件
1: 4-Methylpyridine; n-butyllithium With 2-(dimethylamino)-ethanol in hexane T=0°C; 1 h; 2: dimethyl-disulfide in tetrahydrofuran; hexane T=-78°C; 1 h; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3855 - 3860
反应条件
carbon monoxide in toluene dissolving educt in CO saturated solvent, standing at 23°C; UV/VIS-spectroscopy monitoring; not isolated;
参考文献
Inorganic Chemistry, , vol. 28, p. 2231 - 2234
反应条件
hydrogenchloride in water 0.5 h; Ambient temperaturevariation of pH, temp. and time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 46 p. 6365 - 6368
反应条件
in dichloromethane Irradiation (UV/VIS); photolysis (He-Cd laser, 442 nm, room temp.); HPLC anal., estimation of quantum yield;
参考文献
Inorganic Chemistry, , vol. 28, p. 2281 - 2285
