1.1: 95 percent / t-BuOK / tetrahydrofuran / 9 h / 0 - 20 °C
2.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
2.2: tetrahydrofuran; hexane / 8.5 h / -78 - 20 °C
3.1: 37.09 g / aq. HCl / 3 h
View Scheme
参考文献
Robert, Patricia; Bolduc, Andreanne; Skene, W. G.
Journal of Physical Chemistry A: Molecules, Spectroscopy, Kinetics, Environment, and General Theory, 2012 , vol. 116, # 37 p. 9305 - 9314,10