3,5-二甲氧基苯甲酸合成路线 （共 127 条）
反应条件
sodium in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Azzena, Ugo; Melloni, Giovanni; Piroddi, Anna Maria; Azara, Emanuela; Contini, Stefania; Fenude, Emma
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3101 - 3106
反应条件
1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
CpMo(CO)3(CCPh); dihydrogen peroxide in water T=80°C; 8 h; chemoselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 24 p. 2885 - 2888
反应条件
C36H50NO4V; oxygen in dimethylsulfone; deuterated toluene T=100°C; 48 h;
参考文献
Inorganic Chemistry, , vol. 51, # 13 p. 7354 - 7361
反应条件
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C 2.1: triethylamine; chloro-trimethyl-silane; 4-(N,N-dimethlyamino)pyridine / tetrahydrofuran / 0.25 h / 0 - 20 °C 2.2: 0.5 h / 20 °C / |Cooling with ice 3.1: (8-oxyquinolinate)2VV(O)(OiPr) / pyridine-D5 / 48 h / 100 °C View Scheme
参考文献
ACS Catalysis, , vol. 3, # 12 p. 3111 - 3122
反应条件
potassium permanganate; disodium hydrogenphosphate in water; acetone 3 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 9 p. 3501 - 3517
反应条件
potassium cyanide; water T=80°C; 24 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 6 p. 2070 - 2072
反应条件
1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7451 - 7455
