3,5-二甲氧基苯甲酸合成路线 （共 127 条）
反应条件
LiSEt in N,N-dimethyl-formamide T=20°C; 19 h; Inert atmosphere;
参考文献
Cvengros, Jan; Neufeind, Stefan; Becker, Anne; Schmalz, Hans-Guenther
Synlett, 2008 , # 13 p. 1993 - 1998
反应条件
sodium perborate in acetic acid T=45 - 50°C; 8 h;
参考文献
McKillop, Alexander; Kemp, Duncan
Tetrahedron, 1989 , vol. 45, # 11 p. 3299 - 3306
反应条件
1: in tetrahydrofuran T=20°C; P=3000.3 Torr; gas-liquid flow reactor assembly; 2: With polymer-supported sulfonic acid in tetrahydrofuran
参考文献
Polyzos, Anastasios; O'Brien, Matthew; Petersen, Trine P.; Baxendale, Ian R.; Ley, Steven V.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 5 p. 1190 - 1193
反应条件
sodium hydroxide in water
参考文献
Smidrkal, Jan; Harmatha, Juraj; BudiSinsky, Milo; Vokae, Karel; ZIDEKc, Zdenik; Kmoniekova, Eva; Merkl, Roman; Filip, Vladimir
Collection of Czechoslovak Chemical Communications, 2010 , vol. 75, # 2 p. 175 - 186
反应条件
sodium hydroxide in water T=80 - 90°C; pH=8.5 - 9; 2 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 41, # 11 p. 2395 - 2398
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Lesma, Giordano; Sacchetti, Alessandro; Silvani, Alessandra
Synthesis, 2006 , # 4 p. 594 - 596
反应条件
1: With methanol; copper(II) bis(trifluoromethanesulfonate) T=20°C; 16 h; 2: With Ba(OH)2 in methanol; water T=20°C; 3: With hydrogenchloride in methanol; water
参考文献
Broehmer, Manuel C.; Mundinger, Stephan; Braese, Stefan; Bannwarth, Willi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 27 p. 6175 - 6177
反应条件
silica-supported Jones reagent in dichloromethane 0.035 h;
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.
Tetrahedron Letters, 2006 , vol. 47, # 30 p. 5261 - 5264
反应条件
potassium phosphate; copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
potassium hydroxide T=100°C; solvent-free Cannizzaro reaction; 0.0833333 h;
参考文献
Tetrahedron Letters, , vol. 42, # 45 p. 7983 - 7985
