N-(2,6-二甲基苯基)氯乙酰胺合成路线 (共 36 条)
反应条件
sodium carbonate in dichloromethane T=10 - 15°C; 1.5 h; Large scale reaction;
参考文献
Aalla, Sampath; Gilla, Goverdhan; Anumula, Raghupathi Reddy; Kurella, Srinivas; Padi, Pratap Reddy; Vummenthala, Prabhakar Reddy
Organic Process Research and Development, 2012 , vol. 16, # 5 p. 748 - 754
参考文献
Bhatia, Pramila A.; Daanen, Jerome F.; Hakeem, Ahmed A.; Kolasa, Teodozyj; Matulenko, Mark A.; Mortell, Kathleen H.; Patel, Meena V.; Stewart, Andrew O.; Wang, Xueqing; Xia, Zhiren; Zhang, Henry Q.
Patent: US2004/29887 A1, 2004 ;
反应条件
methyl lithium LiBr complex in diethyl ether T=-78°C;
参考文献
Pace, Vittorio; Castoldi, Laura; Holzer, Wolfgang
Chemical Communications, 2013 , vol. 49, # 75 p. 8383 - 8385
反应条件
in water T=20°C; 2 h;
参考文献
Kommi, Damodara N.; Kumar, Dinesh; Chakraborti, Asit K.
Green Chemistry, 2013 , vol. 15, # 3 p. 756 - 767
反应条件
hydrogenchloride in water 2 h; Heating;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 98, # 5 p. 319 - 326
反应条件
hydrogenchloride in water 5 h; Heatingvariation of catalyst concentration, reaction time; Product distributionMechanism;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 98, # 5 p. 319 - 326
参考文献
Loefgren
Arkiv foer Kemi, 1946 , vol. 22A, # 18 p. 11
反应条件
HCO2Cs in methanol 24 h; RefluxInert atmosphere;
参考文献
Wong, Fung Fuh; Chang, Po-Wei; Lin, Hui-Chang; You, Bang-Jau; Huang, Jiann-Jyh; Lin, Shao-Kai
Journal of Organometallic Chemistry, 2009 , vol. 694, # 21 p. 3452 - 3455