反应条件
1: 68 percent / NaBH4 / tetrahydrofuran; H2O; CH2Cl2 / 42 h / 20 °C 3: 95 percent / HSiCl3 / xylene / 1.) from 0 deg C to RT, 2.) from 100 to 120 deg C, 2 h, 3.) reflux, 3 h View Scheme
参考文献
Matteoli, Ugo; Beghetto, Valentina; Schiavon, Cristina; Scrivanti, Alberto; Menchi, Gloria
Tetrahedron Asymmetry, 1997 , vol. 8, # 9 p. 1403 - 1409