反应条件
2: 62 percent / methyl lithium, phosphorus trichloride, TMEDA / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) -78 to 20 deg C, 90 min, 3.) 20 deg C, 30 min
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参考文献
Baldwin, Jack E.; Adlington, Robert M.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Newington, Ian M.; Perry, Matthew W. D.
Tetrahedron, 1986 , vol. 42, # 15 p. 4235 - 4246